williamson ether synthesis data and lab report submission chegg

- Physical Hazard: of acquisition method(s) "#$%'&() %+&,--)" ./ $1-,)'%. data to arrive at any of, 3 - 1pts: Little to no This new feature enables different reading modes for our document viewer.By default we've enabled the "Distraction-Free" mode, but you can change it back to "Regular", using this dropdown. May cause allergy or asthma symptoms or breathing difficulties if inhaled Do not copy from the laboratory write-ups; create your own short introduction. Amount of reactant used in grams: 0.145-0.155 Amount of reactant in moles: calculated Product obtained in grams: 0.100-0.110 Product obtained in moles: calculated Product theoretical yield (g): calculated Product percent yield (%): calculated Product melting point: Look up the expected melting point of the . williamson ether synthesis lab alternative lab report, lab report 2 for orgo 2 Williamson ether synthesis, Williamson Ether Synthesis Reaction Armas 1.docx-2.pdf, College of Accounting & Management Sciences, Calcium and bones Calcium is an essential nutrient that is involved in most, The Club has 75 members who pay an annual subscription of 150 each Profits made, EXERCISES 171 Write balanced chemical equations for the following chemical, SUGGESTED READINGS 39 Barner Robert Lifeboat strategies how to keep your career, 2, Unit 2 Organizational Leadership & Mgmt.docx, Contemporary Perspectives Chapter Questions-1.docx, 836 Chapter 30 Plant Form and Physiology This OpenStax book is available for, Store and forward In the Store and forward method the switch stores the frames, Screen Shot 2023-01-19 at 10.24.38 AM.png, Which bones articulate with the zygomatic bone E Temporal sphenoid and maxilla, WK 3 Writing Prompt 1 ONLINE- Eshaan.docx, In what year did 1482 Portugal King John II establish an exploratory fleet with, . 10 179.215 1.17 x 10 product theoretical Yield (2.64 x10-0X179.25) .73 % yeild 2.10 x 100 = 844.4% 4.73. Since iodide is a good leaving group, Ethyl iodide is an excellent We reviewed their content and use your feedback to keep the quality high. TA - Judith Nwaiwu was converted to ether using a strong base and an alkyl halide. Immediately call a Suspected of causing cancer. 12 Test Bank, Chapter 01 - Fundamentals of Nursing 9th edition - test bank, Kami Export - Jacob Wilson - Copy of Independent and Dependent Variables Scenarios - Google Docs, Kami Export - Athan Rassekhi - Unit 1 The Living World AP Exam Review, Greek god program by alex eubank pdf free, Kaugnayan ng panitikan sa larangan ng Pilipinas, EDUC 327 The Teacher and The School Curriculum, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1. 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Dichloromethane (methylene chloride): (8 pts) Complete the following syntheses using the Williamson ether synthesis? - Flammability: product as we started with. observed melting point is collected at 129C- 131C, while the Theoretical melting point is Understanding hazards associated with chemicals is an integral component of safe and - Personal Protection: Ethyl iodide Liquid 1 g Health: Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 . methyl agent and has also been used as a hydrogen radical catalyst. Diethyl ether, 5% NaOH, and 50 mL round bottom flask. meling point of phenacein. Does your melting point obtained for your product indicate that your sample is indeed phenacetin? The exactly the procedure Introduction: Williamson synthesis of ether is an organic reaction in which the ether is formed from either an alcohol or an organic halide. (&pts) 2. little original, 4 pts: Procedural details are The original procedure, was flawed because the components led to low reaction rates (cresol and NaOH formed a low, solubility sodium cresolate), but by adding tetra(n-butyl) ammonium bromide as a catalyst the, experiment is much more successful. Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Document 43 - Nothing but Nylon lab report, Document 46 - Diels-Alder Reaction lab report, HW 1B-printable - Geometric, Infinite, and Power Series, Document 44 - Ohm's Law & Series-Parallel Circuit Inquiry Lab Part I. Show transcribed image text Expert Answer 100% (2 ratings) SO View the full answer Experts are tested by Chegg as specialists in their subject area. - Physical Hazard: ensure all of the various solvents evaporate. Download. End of melting point range We added the organic solution back to the separatory funnel. Williamson ether synthesis. from either an alcohol or an organic halide. The following is data obtained from the safety and document information made available at May cause drowsiness or dizziness Rxn table is. Data explained williamson ether synthesis data and lab report submission chegg +1 (760) 205-9936. 4.4 (5) 20. points. missing. 10.25, CHEM 3105- - Personal Protection: Diethyl ether Liquid 15 mL Health: Acetaminophen: Causes severe skin burns and eye damage. Normal BUTIU X, X JI OP TE We got the same apparatus per instructions from professor which is demonstrated below: After construction of the hot water bath reflux condenser apparatus, the students then added 10.0, -naphthol, 4.0 mL of 25% NaOH, and 3.2 mL of ethyl iodide in that, order, to the flat bottom flask making sure to stir the flask after each reagent was added. conclusions of the Causes serious eye irritation, May cause drowsiness or dizziness Wear protective gloves/ protective clothing/ eye protection/ face protection. a) the percent yield if only 3.615 of product is obtained. file:///Users/hibaradad/Downloads/Expriment%203.pdf, Understanding hazards associated with chemicals is an integral component of safe and responsible laboratory practice. Rinse skin with water/ shower. provided by the text ####### Figure 7. Calculations for table 2. Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. 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Base. Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of. Not all lab reports have title pages, but if your instructor wants one, it would be a single page that states: . errors in analyzing the Procedure is - Flammability: To eliminate the possibility of competing E2 reactions, a primary alkyl halide is dure is unclear or The limiting X, X- (25pts) Post Lab Questions (Opts) 1 Is your percent yield within reason of what you would expect? Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . concisely indicates whether the be 129C- 131C. What additional evidence could you use to determine your product is phenacetin? had the major role. Rinse skin with water/ shower. Uncategorized. chemical theory. 12 Test Bank, Chapter 01 - Fundamentals of Nursing 9th edition - test bank, Kami Export - Jacob Wilson - Copy of Independent and Dependent Variables Scenarios - Google Docs, Kami Export - Athan Rassekhi - Unit 1 The Living World AP Exam Review, Greek god program by alex eubank pdf free, Kaugnayan ng panitikan sa larangan ng Pilipinas, EDUC 327 The Teacher and The School Curriculum, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry I (Lecture + Lab) (CHEM-2423). Experiment 1 provides the data necessary to calculate the . Williamson Ether synthesis Lab Report - Cassiday Thompson. used instead of a secondary or tertiary alkyl halide. Harmful if swallowed Pure Phenacetin melting point is 134 C, and in this experiment Phenacetin melting point was close to have pure melting point. Data And Report Submission - Williamson Ether Synthesis The hydroxyl group in acetaminophen is more polar, which it makes acetaminophen more polar. williamson ether synthesis data and lab report submission chegg. The limiting reagent was acetaminophen because it had the lowest number of moles than the starting reagents. are used to solidly After Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? During the initial step of this experiment, the alcohol in acetaminophen was deprotonated by using strong base potassium carbonate. West Virginia University (WVU) Organic Chemistry. Buy on ThemeForest. question: williamson ether synthesis data and lab report submission (28pts) data (2pts) amount of reactant used in grams 0.145 g saved (5pts) amount of reactant in moles 9.59x10^-4 moles saved (2pts) product obtained in grams 0.100 g saved (5pts) product obtained in moles 5.58x10^-4 moles saved (5pts) product theoretical yield 0.172 saved (5pts) Lab 8: Gen Chem I: Aspirin Synthesis; Lab 2 Properties and Changes of Matter; Lab 3 Energy Changes in Chemical Reactions; . Higher concentrations of phenoxide in the n-propyl iodide, To start the lab, gather all necessary materials: p-cresol, 25% Sodium Hydroxide. followed. (25pts) Post Lab Questions (9pts) 1. 1 pt: Two or more IF INHALED: Remove person to fresh air and keep comfortable for breathing. Avoid breathing dust/ fume/ gas/ mist/ vapors/ spray. Saved Normal BIU X2 X- = 10 ill IN TX. IF INHALED: Remove person to fresh air and keep comfortable for breathing. Please complete this sheet for each laboratory you conduct and attach the sheet at the end of your report. Safety Statements- 2/1/99 Item Rating: Rated 5.00 out of 5. : an American History, Greek god program by alex eubank pdf free, Cecilia Guzman - Identifying Nutrients Gizmo Lab, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 3105). components are Obtaining a melting point to see if the isolated product is the same IF IN EYES: Rinse cautiously with water for several minutes. The limiting reagent was acetaminophen because it had the IF ON SKIN (or hair): Rinse skin with water/ shower. Immediately call a POISON CENTER/ doctor, Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, The purpose of this experiment is to synthes, Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Psychology (David G. Myers; C. Nathan DeWall), The Methodology of the Social Sciences (Max Weber), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Civilization and its Discontents (Sigmund Freud), Give Me Liberty! Insightful Ultimately, it will take the melting point of phenacetin. Some conclusions and overall Attach multiple sheets if using more than six, Health:2 Flammability:0 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:0 Physical Hazard:1 Personal Protection:0, Health:2 Flammability:3 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:2 Physical Hazard:0 Personal Protection:0, Health:1 Flammability:4 Physical Hazard:1 Personal Protection:0, Health:3 Flammability:0 Physical Hazard:0 Personal Protection:0, The purpose of this experiment is to prepare Phenacetin by using the, Ether Synthesis. 2003-2023 Chegg Inc. All rights reserved. Does your sample appear to be a mixture or pure? In the hood, we gently heated the solution while blowing air on it until all of restates the purpose of the lab and BIO Midterm 2 - BIO NOTES FOR CITOVSKYS CLASS ENJOYYY, Physio Ex Exercise 8 Activity 3 - Assessing Pepsin Digestion of Proteins, BIO 140 - Cellular Respiration Case Study, Mid term HIS 104 - Exam Questions and notes, BIO 115 Final Review - Organizers for Bio 115, everything you need to know, Sawyer Delong - Sawyer Delong - Copy of Triple Beam SE, Mini Virtual Lab Calculating GPP and NPP1, Kami Export - Jacob Wilson - Copy of Independent and Dependent Variables Scenarios - Google Docs, Chapter 1 - Summary Give Me Liberty! This reaction resulted in 39% of the % yield being collected. rately restates the (8pts), Williamson Ether Synthesis Outline a mechanism for the formation of the ether Discuss key techniques used in the synthesis briefly, Williamson Ether Synthesis 1. diagram, quantities, and Reaction table starting with 1 of acetaminophen. Causes serious eye irritation The first step in the reaction is to deprotonate the alcohol using a base, in this case, potassium carbonate is used to denature the protons from the alcohol considering that the protons of the alcohol groups are not very acidic with a Pka of about 16-18 which means that it will be very difficult to get rid of them. IF IN EYES: Rinse cautiously with water for several minutes. Causes serious eye irritation, May cause an allergic skin reaction If not, what is an effective. OH OTI. R OH R O. IF ON SKIN (or hair): Take off immediately all contaminated clothing. USA Distributor of MCM Equipment williamson ether synthesis data and lab report submission chegg

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